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Facile synthesis of aluminum oxyhydroxide-PVA films and its adsorptive evaluation for the removal of methylene blue dye from water: kinetics, optimization studies and mechanism
Aluminum oxyhydroxide-polyvinyl alcohol films were synthesized by the solgel method with varying metal-polymer ratios. The results of the characterization confirmed the formation of aluminum oxyhydroxideand the incorporation of metal into the polymer. The adsorption isotherms of the film exhibited type IV isotherms indicating the mesoporous nature with a non-uniform pore size distribution. The optical profilometric studies confirmed the surface roughness of the film. The adsorptive nature of the film was tested for the removal of methylene blue dye from the aqueous solution. Optimization studies were conducted to investigate the effect of various parameters on the adsorption process. The adsorption isotherms of methylene blue fit with the Langmuir isotherm model and follow a pseudo-second-order equation. A suitable reaction mechanism was proposed, which confirms the adsorptive nature of the film is due to the electrostatic attraction. The synergetic effect of the metal-polymer blend, surface roughness and pore size of the film, which ranges from 0.01 to 0.025nm,enhances the adsorption of methylene blue. The comparison of results obtained in the current study with earlier reports confirms that the aluminum oxyhydroxide-polyvinyl alcohol films can be considered an eco-friendly, cost-effective adsorbent for removing methylene blue. 2023, The Polymer Society, Taipei. -
Facile synthesis of Bi2WO6-NiO nanocomposite for supercapacitor application
In order to prepare for future high-power storage-related applications, a tremendous amount of studies have been conducted on the manufacturing of high-performance supercapacitor electrodes. The hydrothermal technique was used to synthesize Bi2WO6NiO nanocomposite (NC), which was examined using FTIR, XRD, HR-TEM, EDX, FESEM, and XPS techniques. Furthermore, the Bi2WO6-NiO NC performs with an elevated specific capacity of 398.2C/g at 10 mV/s. The charge transfer resistance (Rct) and solution resistance (Rs) of Bi2WO6-NiO NC were determined as 0.81 and 0.23 ? using electrochemical impedance spectra (EIS). Bi2WO6-NiO NC extended the chargedischarge time and rate capacities, as shown by the galvanostatic chargedischarge (GCD) analysis. Even after 2000 cycles, Bi2WO6-NiO NC cyclic stability was superior with a capacitive retention of 89.3 %. A power density of 6750 W/kg resulted from the constructed asymmetric supercapacitor (ASC) device based on Bi2WO6-NiO/AC, exhibiting an energy density of 32.5 Wh/kg. Additionally, the ASC maintains high cyclic stability with 90.8 % of initial capacity, even after 2000 chargedischarge cycles in a row. 2024 Elsevier B.V. -
Facile Synthesis of Few-Layer Graphene Oxide from Cinnamomum camphora
Abstract: This study presents a facile synthesis technique to produce few-layer graphene oxide from Cinnamomum camphora (Camphor L.). Camphor upon carbonization and chemical oxidation leads to the formation of few-layer graphene oxide sheets of around ten layers with a lateral size of 4.14 nm and stacking height of 3.10 nm. AFM and SEM analysis results reveal the wrinkled morphology of the graphene oxide sheets formed. The sharp G band and the relative intensity of the defect to the graphitic band in the Raman spectrum indicate the formation of nanocrystalline graphene oxide sheets with fewer defects. The FTIR spectrum and the deconvoluted C 1s XPS spectrum of graphene oxide synthesized reveal the presence of predominant sp2 hybridized carbon along with carbon bound to various oxygen functionalities. In brief, the formation of high-quality few-layer graphene oxide from an abundant, low-cost, and readily available botanical precursor is herein reported. 2021, Pleiades Publishing, Ltd. -
Facile synthesis of graphene-tin oxide nanocomposite derived from agricultural waste for enhanced antibacterial activity against Pseudomonas aeruginosa
Antibacterial screening of graphene-tin oxide nanocomposites synthesized from carbonized wood and coconut shell is investigated against Pseudomonas aeruginosa for the first time. Efficient and facile one step hydrothermal process adopted in the present work for the synthesis of graphene-tin oxide nanoparticles provides an ideal method for the economic large-scale production of the same. Graphene-tin oxide nanocomposites derived from wood charcoal possess a spherical morphology whereas rod like structures are seen in the case of coconut shell derivatives. An excitation independent fluorescence response is observed in graphene-tin oxide nanohybrids while graphene oxide nanostructures exhibited an excitation dependent behavior. These hydrophilic nanostructures are highly stable and exhibited no sign of luminescence quenching or particle aggregation even after a storage of 30 months. Bactericidal effects of the nanostructures obtained from coconut shell is found to be relatively higher compared to those procured from wood. This variation in antibacterial performance of the samples is directly related to their morphological difference which in turn is heavily influenced by the precursor material used. MIC assay revealed that coconut shell derived graphene-tin oxide composite is able to inhibit the bacterial growth at a lower concentration (250 ?g/mL) than the other nanostructures. Nanocomposites synthesized from agro-waste displayed significantly higher antimicrobial activity compared to the precursor and graphene oxide nanostructures thereby making them excellent candidates for various bactericidal applications such as disinfectants, sanitary agents etc. 2019, The Author(s). -
Facile synthesis of Mn-Ni bimetal organic framework decorated with amine as an electrode for a high-performance supercapacitor
In the recent years, the whole world is looking for better energy storage devices. Supercapacitors are among the mostpromising high-capacity energy storage devices. Manganese-based material has gained more importance among transition metals due to its cost, easy fabrication, and wide potential applications. Here, we report the synthesis of a novel MOF using metal centers, dicarboxylate ligand, and aminoterephthalic acid as a co-ligand {Mn-Ni-NH2(h2fipbb)}MOF. The synthesized material has a unique hierarchical morphology consisting of manganese and nickel connected with NH2 through h2fipbb ligand linkage, which is highly efficient for the permeation of the electrolyte and electron transfer. The {Mn-Ni-NH2(h2fipbb)}MOF shows an excellent specific capacitance of 711.60 F g?1 using 2M KOH at a current density of 1 A g?1. The two electrode system material exhibitsa high-power and energy density of 743.99Wkg?1 and 20.49 Wh kg?1, respectively. From the above results, the synthesized {Mn-Ni-NH2(h2fipbb)}MOF can be considered a promising material for electrochemical energy storageapplications. 2023, The Author(s), under exclusive licence to Springer-Verlag GmbH Germany, part of Springer Nature. -
Facile synthesis of nickel nanoparticles and its efficient dye degradation
The present investigation involves the synthesis of nickel (Ni) nanoparticles (NPs) by the chemical reduction of nickel chloride using hydrazine hydrate without the need for an inert atmosphere from an external source. The photocatalytic activity, structure and morphology of the NPs were studied by employing UV-Visible (UV-Vis) spectroscopy, powder X-ray diffraction (PXRD) and transmission electron microscopy (TEM). Degradation of methylene blue(MB) and rhodamine B(Rh-B) dyes using Ni NPs was investigated to see the feasibility in degrading these dyes from polluted water at low cost. Ni NPs showed a good photocatalytic activity of 84.1% under visible light for the degradation of MB when compared to Rh-B which showed an efficiency of 47.3 %. 2020 World Research Association. All rights reserved. -
Facile synthesis of novel antimony selenide nanocrystals with hierarchical architecture by physical vapor deposition technique
Stoichiometric antimony selenide (Sb 2 Se 3 ) nanocrystals have been successfully engineered by a facile physical vapor deposition method, employing a single precursor of polycrystalline Sb 2 Se 3 charge in a closed quartz ampoule under high vacuum without any foreign seed or extraneous chemical elements. This work underscores the efficacy of the vapor deposition process and provides synthetic strategies to scale down bulk Sb 2 Se 3 into novel nanostructures. The morphological evolution of the tailored architecture was examined on micro and nano size scales by scanning electron microscopy and high-resolution transmission electron microscopy. The intrinsic mechanism governing the nanostructure formation is revealed as layer-by-layer growth, related to the unique layered structure of Sb 2 Se 3 . The optical properties of the grown crystals were probed by UVvisNIR and photoluminescence tools. The band-gap values of the microfibers, nanorods, nanooctahedra and nanospheres estimated from UVvisNIR analysis are found to be 1.25, 1.47, 1.51 and 1.75 eV, respectively. Powder X-ray diffraction, energy-dispersive analysis by X-rays, X-ray photoelectron spectroscopy, Raman spectroscopy and photoluminescence studies confirmed the quality, phase purity and homogeneity of the as-grown nanostructures. The adopted physical vapor deposition method is thus shown to be a simple and elegant route which resulted in the enhancement of the band gap for the Sb 2 Se 3 samples compared with their counterparts grown by chemical methods. This approach has great potential for further applications in optoelectronics. International Union of Crystallography, 2019 -
Facile synthesis of novel SrO 0.5:MnO 0.5 bimetallic oxide nanostructure as a high-performance electrode material for supercapacitors
Perovskite bimetallic oxides as electrode material blends can be an appropriate method to enhance the supercapacitor properties. In the present research, SrO 0.5:MnO 0.5 nanostructures (NS) were synthesized by a facile co-precipitation method and calcinated at 750800C. Crystal structure of SrO 0.5:MnO 0.5 NS were characterized by X-ray diffraction, surface chemical composition and chemical bond analysis, and dispersion of SrO into MnO was confirmed by X-ray photoelectron spectral studies. Structural morphology was analyzed from scanning electron microscopy. Optical properties of SrO 0.5:MnO 0.5 NS were studied using UV-Visible spectrophotometer and SrO 0.5 and MnO 0.5 NS showed ?75nm grain, ? 64nm grain boundary distance, with two maxima at 261nm and 345nm as intensity of absorption patterns, respectively. The synthesized SrO 0.5:MnO 0.5 NS exhibited high specific capacitance of 392.8F/g at a current density of 0.1A/g. Electrochemical impedance spectroscopy results indicated low resistance and very low time constant of 0.2s ?73% of the capacitance was retained after 1000 galvanostatic charge-discharge (GCD) cycles. These findings indicate that SrO 0.5:MnO 0.5 bimetallic oxide material could be a promising electrode material for electrochemical energy storage systems. The Author(s) 2022. -
Facile synthesis of preformed mixed nano-carbon structure from low rank coal
Coal is a natural energy resource which is mainly used for energy production via combustion. Coal has nanocrystals embedded in it, formed during the coalification process, and is an ideal precursor for nano-carbon dots and diamonds. Herein, we report a facile top-down method to synthesise nanodots and diamonds of the size of 5 nm to 10 nm from three different types of coal by simple chemical leaching. TEM analysis revealed the formation of a mixture of carbon dots, graphene layers, and quantum dots in bituminous coal and sub-bituminous coal. Raman analysis confirmed the existence of synthesized nano-diamond and nano-carbon mixed phase with defects associated with it. It is concluded that graphene quantum dots, nano-diamonds, graphene sheets and carbon dots present in coal can be extracted by simple chemical treatment. These structures can be tuned to photoluminescent material for various optoelectronic applications or energy harvesting devices like super capacitors. 2018. This is an open access article distributed under the Creative Commons Attribution-NonCommercial-NoDerivatives 3.0 License. -
Facilitating Faculty Development for Training in Multicultural Competence in Health Service Psychology Graduate Programs Through an International Collaboration
A critical aspect of strengthening graduate-level clinical and counseling psychology training in cultural competence is to build capacity among faculty teaching in these programs to provide effective training. We addressed this need through an international collaboration between a university in India and another in the United States that included faculty travel to another country, peer mentoring groups, and review of curricula. This article describes faculty perceptions of this program and its perceived impact on their professional development and outlines curricular and research outcomes that resulted from the program. Across 4 years, a total of eight faculty visits took place with Indian faculty (n = 13) visiting the United States and US faculty (n = 11) visiting India. After each visit, faculty at both institutions responded to open-ended questions about the usefulness of these visits and completed a rating scale at the end of the program through an online survey. Faculty from both countries indicated that the visits contributed to enhanced cultural awareness and sensitivity by broadening their perspectives and learning about cultural similarities and differences. Indian faculty described learning about new pedagogical methods and enhanced motivation to engage in research and publish, along with new collaborative opportunities. US faculty described incorporating cultural competence more centrally in their teaching and clinical supervision through increased commitment, as well as inclusion of more global and diverse content and assignments aimed to increase students cultural competence. These responses provide preliminary support for the usefulness of cultural immersion experiences for faculty professional development. 2024 American Psychological Association Inc.. All rights reserved. -
Factor investing: evidence of long-only factor portfolios from the Indian market
The study examines the performance of long-only factor portfolios in the Indian market. An extended 8-factors model and well-known factor models are used to analyse the exposure and risk-adjusted performance of factor portfolios. The results reveal a mixed portfolio performance: market-driven factors like illiquid, winner, stable, and small offered better performance than those based on fundamental data like value, strong, and conservative. While the market factor is the primary return driver, the SMB and HML factors are the other standard return drivers. The portfolios showed exposure to the specific factor they are constructed upon, except for the strong portfolio. 2024 Informa UK Limited, trading as Taylor & Francis Group. -
Factors Affecting Consumer Buying Behaviour, Consumer Satisfaction and Consumer Loyalty in the Ghee Industry- A Perspective of Bangalore Ghee Market
Asian Journal of Research in Business Economics and Management, Vol. 7, Issue 2, pp. 18-34, ISSN No. 2249- 7307 -
Factors Affecting Digital Visibility of Small and Medium Enterprises in India
This study sketches the importance of social media, integrated marketing communication, social customer relationship management and its transformation in the small and medium enterprises (SME). These factors can increase interaction and communication of SMEs with its customers. This study incorporates empirical method to elaborate how SMEs can increase visibility and reachability by gaining value through the usage of social media. Findings of the study highlight the challenges faced by SMEs with respect to visibility, examines the usage of different digital platforms by Indian SMEs which can resolve these difficulties and its impact on the business for improved visibility of SMEs when competition is hitting hard on all businesses. 2021 Management Development Institute. -
Factors Affecting Intra-Relations of Backend Cost Drivers in Multi-Brand Retail Domestic Super Market Under Convenience Stores Format : A Customer Aligned Model of Supply-Chain Optimism Framework
Asian Journal of Management, Vol. 8, Issue 1, pp. 78-86, 2321-5763 -
Factors affecting intra-relations of backend cost drivers in multi-brand retail domestic super market under convenience stores format: A customer aligned model of supply-chain optimisation framework /
Asian Journal Of Management, Vol.8, Issue 1, pp.78-86, ISSN: 0976-495X (Print), 2321-5763 (Online). -
FACTORS AFFECTING ORGANIC FARMING CULTIVATION AND THEIR ROLE IN ACHIEVING SUSTAINABLE DEVELOPMENT GOALS (SDG)
Objectives: The paper aims to explore the factors which influence the organic farming cultivation in India and how they lead towards attainment of SDG. Theoretical Framework: This paper has adopted Theory of Planned Behavior to identify the factors which influence the organic farming and define their relationship with SDG. Method: The paper attempts to explore the factors which influence the organic farming intention among the farmers. It further explores the relationship between intention for organic farming and adoption of organic farming. The data was captured through detailed questionnaire which was captured through 347 respondents. The data analysis was performed with the help of SPSS 29 and AMOS 29 The mediating role of motivation was also explored using process Macro 4.2. Results & Discussions: The findings revealed that environment and cost influence the organic farming intention while attitude and perception had no effect on organic farming intention. Adoption of organic farming shared a positive relationship with organic farming intention The Cultivation of organic products lead to attainment of following goals No Poverty (SDG 1), zero Hunger (SDG2), Good Health and Well Being (SDG3) and Responsible Consumption and Production (SDG 12). Research Implications: The study reveals that there is a need to raise the awareness level among the farmers regarding the role of organic farming, its environmental impacts and health benefits associated with it. The findings underscore the importance of implementing additional training and awareness programs targeted at novice and less-experienced farmers. Such initiatives aim to familiarize them with diverse aspects of marketing, economics, and social factors associated with organic farming. 2025, Editora Alumni In. All rights reserved. -
Factors affecting the competitive capability of small and medium women entrepreneurs
Small and medium women entrepreneurs have a major contribution in the countrys economic development. After the implication of liberalization, privatization and globalization, all the countries are paying attention to support small and medium women entrepreneurs in order to mobilize maximum resources, generate employment opportunities and to improve competitiveness among them. However, today women entrepreneurs are still facing many problems in terms of finance, human resources, marketing, technology capability etc. These capabilities will result in the development of competitive capability of small and medium women entrepreneurs. Competitive capability is very important in order to sustain not only in the local market but also in the national and international market. Therefore, this study is an attempt to explore the factors affecting the competitive capability of small and medium women entrepreneurs. This study is surveyed 400 women entrepreneurs and obtained complete response from 384women entrepreneurs with 23 questions. The data is collected from November 2019 to January 2020. Simple random sampling technique, Cronbach's alpha and Structural Equation Modelling (SEM) technique are used in the study to obtain the research result. Finally, the study concludes that there are five factors that affect the competitive capability of small and medium women entrepreneurs with significance level 0.05 and the influence of technology capability is more compare to other capabilities on competitiveness of the women entrepreneurs. 2020 SERSC. -
Factors Affecting the Performance of Private Label Brands in Indian Online Market: An Assessment of Reliability and Validity
Asian Journal of Management, Vol. 7, Issue 3, pp. 223-230, ISSN No. 0973-8705 -
Factors Affecting the Risk Perceptions of Cryptocurrency Investors
This study explores risk perceptions in cryptocurrency investments among Indian investors. It employs a multistage random sampling survey of 228 investors. Four key factors influence this perception: conceptual clarity, investment education, awareness of investment options, and fear-induced psychological factors. The overall risk perception of crypto investors is high. Based on our findings, we suggest that the Indian government should organize an awareness campaign to create awareness and educate investors about cryptocurrency. Policymakers and investment managers should focus on transforming high-risk investors into lower-risk investors through education and support, fostering a more favorable investment environment. 2024 The Institute of Behavioral Finance. -
Factors effecting employees willingness to stay in information technology industry /
The International Journal of Nepalese Academy of Management, Volume 1, Issue 1, pp.284-303, 2091-2471 (Print), 2091-248X (Online)