Dublin Core The Dublin Core metadata element set is common to all Omeka records, including items, files, and collections. For more information see, http://dublincore.org/documents/dces/. Title A name given to the resource Faculty Publications Article Faculty Publications -Articles Dublin Core The Dublin Core metadata element set is common to all Omeka records, including items, files, and collections. For more information see, http://dublincore.org/documents/dces/. Creator An entity primarily responsible for making the resource Merin Robert, Riya; Jayan, Krishnapriya; Cherian, Tom; Varghese, Anitha Title A name given to the resource High Performance Ferrocene Immobilized Electrodes for the Synthesis of 3-Acetyl Coumarin: A Sustainable Approach Date A point or period of time associated with an event in the lifecycle of the resource 01-01-2025 Source A related resource from which the described resource is derived Journal of the Electrochemical Society;Volume;172;Issue;9;Article No.;96506; Identifier An unambiguous reference to the resource within a given context <a href="https://doi.org/10.1149/1945-7111/ae096a" target="_blank" rel="noreferrer noopener">https://doi.org/10.1149/1945-7111/ae096a</a> <br /><br /><a href="https://www.scopus.com/pages/publications/105017729367?origin=resultslist" target="_blank" rel="noreferrer noopener">https://www.scopus.com/pages/publications/105017729367?origin=resultslist</a> Coverage The spatial or temporal topic of the resource, the spatial applicability of the resource, or the jurisdiction under which the resource is relevant Merin Robert R., Department of Chemistry, CHRIST (Deemed to be University), Bangalore, 560029, India; Jayan K., Department of Chemistry, CHRIST (Deemed to be University), Bangalore, 560029, India; Cherian T., Department of Chemistry, Christ (Autonomous), Kerala, Irinjalakkuda, 680125, India; Varghese A., Department of Chemistry, CHRIST (Deemed to be University), Bangalore, 560029, India Description An account of the resource An electrocatalyst was developed for the synthesis of 3-acetyl coumarin, a known anticoagulant, anti-inflammatory, and anti-microbial compound, by constructing and employing an electrocatalyst with immobilized ferrocenyl aniline onto electro-polymerized anthranilic acid, on a carbon fiber paper electrode. The effectiveness of the modified carbon fiber paper electrode was assessed by analyzing its physicochemical and electrochemical properties, using optical profilometry, field-emission scanning electron spectroscopy (FE-SEM), Fourier-transform infrared spectroscopy (FT-IR), X-ray photoelectron spectroscopy (XPS), cyclic voltametric techniques and electrochemical impedance spectroscopy (EIS) respectively. 3-acetyl coumarin was synthesized using salicylaldehyde and ethyl acetoacetate as starting materials in the presence of piperidine, with lithium perchlorate as supporting electrolyte and ethanol as solvent, at potentiostatic conditions. The reaction was carried out in a three-electrode, single compartment system, at ambient conditions for three hours by using a constant potential of ?1.4 V. The product was purified by column chromatography and characterized by using gas chromatography-mass spectrometry (GC-MS) and proton nuclear magnetic resonance spectroscopy (1H-NMR). The developed electrode was found to be highly efficient towards the synthesis of 3-acetyl coumarin with a good yield of 78%, thereby proving the efficiency and selectivity of the process. 2025 The Electrochemical Society (ECS). Published on behalf of ECS by IOP Publishing Limited. All rights, including for text and data mining, AI training, and similar technologies, are reserved. Subject The topic of the resource 3-acetyl coumarin; conducting polymer; electro-polymerization; electrochemical synthesis; ferrocenyl aniline Publisher An entity responsible for making the resource available Institute of Physics Relation A related resource ISSN: 134651; CODEN: JESOA Language A language of the resource English Type The nature or genre of the resource Article Rights Information about rights held in and over the resource Restricted Access; Hardcopy may be available in the library Format The file format, physical medium, or dimensions of the resource online